Determination of PFAS from Food according to FDA Method C-010.02
Determination of PFAS from Food according to FDA Method C-010.02
Determination of PFAS from Food according to FDA Method C-010.02
Determination of PFAS from Food according to FDA Method C-010.02
Determination of PFAS from Food according to FDA Method C-010.02
- Application Number
- 129000
- Method
- HPLC
- Results
.JPG "null")
Legend: - a = milk - b = curd cheese - c = brussels sprouts - d = spinach - e = bread - f = egg
- Substances
- PFAS: PFBA (Perfluorobutanoic acid); PFPeA (Perfluoropentanoic acid); HFPO-DA (2,3,3,3-Tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy) propanoic acid (GenX)); FBSA (Perfluorobutanesulfonamide); L-PFBS (Perfluorobutanesulfonic acid); PFHxA (Perfluorohexanoic acid); 4:2 FTS (Sodium 1H,1H,2H,2H-perfluorohexanesulfonate); L-PFPes (Perfluoropentanesulfonic acid); PFHpA (Perfluoroheptanoic acid); NaDONA (Sodium dodecafluoro-3H-4,8-dioxanonanoate); FHxSA (Perfluorohexanesulfonamide); PFHxSK (Perfluorohexanesulfonic acid); PFOA (Perfluorooctanoic acid); 6:2 FTS (Sodium 1H,1H,2H,2H-perfluorooctanesulfonate); PFHpS (Perfluoroheptanesulfonic acid); PFNA (Perfluorononanoic acid); FOSA (Perfluorooctanesulfonamide); PFOSK (Perfluorooctanesulfonic acid); PFDA (Perfluorodecanoic acid); 8:2 FTS (Sodium 1H,1H,2H,2H-perfluorodecanesulfonate); 9Cl-PF3ONS (Potassium 9-chlorohexadecafluoro-3-oxanonane-1-sulfonate); L-PFNS (Sodium perfluorononanesulfonate); PFUdA (Perfluoroundecanoic acid); N-MeFOSAA (N-methylperfluorooctanesulfonamidoacetic acid); N-EtFOSAA (N-ethylperfluorooctanesulfonamidoacetic acid); PFDS (Sodium perfluorodecanesulfonate); PFDoA (Perfluorododecanoic acid); 11Cl-PL3OUdS (11-chloroeicosafluoro-3-oxaundecane-1-sulfonic acid); PFTrDA (Perfluorotridecanoic acid); PFTeDA (Perfluorotetradecanoic acid; M4PFBA (Perfluoro-(13C4)butanoic acid); M5PFPeA (Perfluoro-(13C5)pentanoic acid); M3PFBS (Sodium perfluoro-(2,3,4-13C3)butanesulfonate); M5PFHxA (Perfluoro-(1,2,3,4,6-13C5)hexanoic acid); M2-4:2FTS (Sodium 1H,1H,2H,2H-perfluoro(1,2-13C2)hexanesulfonate); M4PFHpA (Perfluoro-(1,2,3,4-13C4)heptanoic acid); M3PFHxS (Sodium perfluoro-(1,2,3-13C3)hexanesulfonate); M8PFOA (Perfluoro-(13C8)octanoic acid); M2-6:2FTS (Sodium 1H,1H,2H,2H-perfluoro(1,2-13C2)octanesulfonate); M9PFNA (Perfluoro-(13C9)nonanoic acid); M8FOSA (Perfluoro-(13C8)octanesulfonamide); M8PFOS (Sodium perfluoro-(13C8)octanesulfonate; M6PFDA (Perfluoro-(1,2,3,4,5,6-13C6)decanoic acid; M2-8:2FTS (Sodium 1H,1H,2H,2H-perfluoro(1,2-13C2 )decanesulfonate); M7PFUdA (Perfluoro-(1,2,3,4,5,6,7-13C7)undecanoic acid); d3-N-MeFOSAA (N-methyl-d3-perfluorooctanesulfonamidoacetic acid); d5-N-EtFOSAA (N-ethyl-d5-perfluorooctanesulfonamidoacetic acid); MPFDoA (Perfluoro-(1,2-13C2)dodecanoic acid); M2PFTeDA (Perfluoro-(1,2-13C2 )tetradecanoic acid)
- Product(s)
Phase REF Webshop NUCLEODUR PFAS
760666.20
NUCLEODUR PFAS Delay
760673.20
- Matrix
- food
- Sample(s)
For sample preparation see MN application 306840
- Conditions
- Eluent A: 5 mM ammonium acetate in water
- Eluent B: 5 mM ammonium acetate in methanol
- Gradient: hold 40 % B for 1 min, in 8 min from 40 % B to 95 % B, hold 95 % B for 3 min, in 0.1 min to 40 % B, hold 40 % B for 2.9 min
- Flow rate: 0.3 mL/min
- Temperature: 40 °C
- Injection volume: 1 μL
- Detection
- MS (see Note)
- Note
- MS conditions - Acquisition mode: SRM - Interface: ESI - Polarity: negative - Curtain Gas: 30 - Collision Gas: medium - Ionspray Voltage: -4500 V - Temperature: 400 °C - Ion Source Gas 1: 50 - Ion Source Gas 2: 60 - Detection Window: 60 sec For more details (e.g., MRM transitions ), check out: www.mn-net.com/pfas
- Author
- Application department
- Source
- MACHEREY-NAGEL, Germany 2022
- Disclaimer
- Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products. MACHEREY-NAGEL does not warrant the correctness of the applications.
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