Analysis of algal toxins in mussels on NUCLEOSHELL Biphenyl compared with NUCLEODUR π2

Analysis of algal toxins in mussels on NUCLEOSHELL Biphenyl compared with NUCLEODUR π2

Analysis of algal toxins in mussels on NUCLEOSHELL Biphenyl compared with NUCLEODUR π2

Application Number
128860
Method
HPLC
Results
null

Legend: - 1) NUCLEOSHELL Biphenyl, 2.7 µm, 150x3 mm - 2) NUCLEODUR π², 5 µm, 250x2 mm

null

Substances
okadaic acid; dinophysistoxin-2; dinophysistoxin-1; pectenotoxin-2
Product(s)
PhaseREFWebshop

NUCLEOSHELL Biphenyl

763636.30

NUCLEODUR π2

760625.20

Matrix
-
Sample(s)

10.0 ng/mL for each analyte

Conditions
  • Eluent A: 50 mmol/L formic acid
  • Eluent B: methanol
  • Gradient: hold 79 % B for 4.0 min, in 0.1 min to 83 % B, in 10.9 min to 86 % B, in 0.1 min to 98 % B, hold 98 % B for 2.9 min, in 0.1 min to 79 % B
  • Flow rate: 0.30 mL/min
  • Temperature: 40 °C
  • Injection: 10 µL
Detection
MS, MRM
Note
Improved peak shape and better baseline separation with core-shell phase NUCLEOSHELL Biphenyl in comparison to NUCLEODUR π² based on fully porous particles.
Author
Helle, N.; Chmelka, F.
Source
TeLA GmbH, Geestland, Germany 2018
Disclaimer
Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products. MACHEREY-NAGEL does not warrant the correctness of the applications.
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