Analysis of nitrosamines by LC-MS/MS
Analysis of nitrosamines by LC-MS/MS
Analysis of nitrosamines by LC-MS/MS
Analysis of nitrosamines by LC-MS/MS
Analysis of nitrosamines by LC-MS/MS
- Application Number
- 128360
- Method
- HPLC
- Results
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- Substances
- N-nitrosodimethylamine; N-nitrosodiethylamine; N-nitrosodi-n-propylamine; N-nitrosodiethanolamine; N-nitrosodi-n-butylamine; 1-nitrosopiperidine; nitrosomorpholine
- Product(s)
Phase REF Webshop NUCLEODUR π2
760636.20
- Matrix
- Sample(s)
100 ng/mL each in water
- Conditions
Eluent A: 0.1 % formic acid in water Eluent B: 0.1 % formic acid in methanol Gradient: hold 2.5 % B for 1.0 min, in 1 min from 2.5 % to 50 % B, hold for 1.0 min, in 0.5 min to 97.5 % B, hold for 2.5 min, in 0.1 min to 2.5 % B, hold for 3.0 min Flow rate: 0.3 mL/min Temperature: 40 °C Injection volume: 20 µL
- Detection
- MS/MS, Sciex API 5500 Ion source: Turbo Spray (APCI) Polarity: positive Scan type: MRM Curtain gas: 35 psig Nebulizer current: 3.0 µA Temperature: 450 °C Gas 1 (nebulizer): 45 psig CAD gas: medium
- Note
- Author
- Application department
- Source
- MACHEREY-NAGEL, Germany 2017
- Disclaimer
- Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products. MACHEREY-NAGEL does not warrant the correctness of the applications.
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