Analysis of pharmaceuticals on core-shell phase with LC-MS/MS detection
Analysis of pharmaceuticals on core-shell phase with LC-MS/MS detection
Analysis of pharmaceuticals on core-shell phase with LC-MS/MS detection
Analysis of pharmaceuticals on core-shell phase with LC-MS/MS detection
Analysis of pharmaceuticals on core-shell phase with LC-MS/MS detection
- Application Number
- 128200
- Method
- HPLC
- Results
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- Substances
- amitriptyline; atenolol; atropine; carbamazepine; chlorpheniramine; clomipramine; diphenhydramine; indapamide; ketamine; ketoprofen; nortriptyline; propanolol; sulfachloropyridazine; sulfadoxine; sulfamerazine; sulfamethoxazole; sulfapyridine; sulfaquinoxaline; trimipramine; verapamil
- Product(s)
Phase REF Webshop NUCLEOSHELL PFP
763532.20
- Matrix
- -
- Sample(s)
For an enrichment from serum by SPE see MN Appl. No. 306510 Sample in 1 mL dest. water - acetonitrile (95:5, v/v)
- Conditions
Eluent A: dest. water + 0,1 formic acid Eluent B: acetonitrile + 0,1 formic acid Gradient: 5 - 95 % B in 7.5 min, 95 % B for 1 min, 95 - 5 % B in 0.5 min, 5 % B for 5 min Flow rate: 0.30 mL/min Temperature: 30 °C Injection volume: 5 µL
- Detection
- LC-MS/MS: AB Sciex API 5500, ion source: Turbo Spray (ESI), scan type: SRM, polarity: positive, curtain gas: 40 psig, ion spray voltage: 5500 V, temperature: 500 °C, gas 1 (nebulizer): 45 psig, gas 2 (turbo gas): 45 psig, collision gas: medium
- Note
- Author
- SPE department
- Source
- MACHEREY-NAGEL, Germany 2017
- Disclaimer
- Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products. MACHEREY-NAGEL does not warrant the correctness of the applications.
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