Analysis of pesticides on core-shell phase with LC-MS/MS detection
Analysis of pesticides on core-shell phase with LC-MS/MS detection
Analysis of pesticides on core-shell phase with LC-MS/MS detection
Analysis of pesticides on core-shell phase with LC-MS/MS detection
Analysis of pesticides on core-shell phase with LC-MS/MS detection
- Application Number
- 128150
- Method
- HPLC
- Results
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- Substances
- acetamiprid; atrazine; azoxystrobin; carbaryl; chlortoluron; chlorpyrifos; clofentezine; clothianidin; coumaphos; cyanazine; desethylatrazine; desisopropylatrazine; diazinon; difenoconazole; diuron; ethoprophos; hexazinone; imazalil; imidacloprid; isoproturon; linuron; methabenzthiazuron; methomyl; metobromuron; metolachlor; monolinuron; myclobutanil; phosalone; piperonylbutoxide; propazine; propyzamide; terbuthylazine; thiacloprid
- Product(s)
Phase REF Webshop NUCLEOSHELL PFP
763532.20
- Matrix
- Sample(s)
For an enrichment from serum by SPE see MN Appl. No. 306360 Sample in 1 mL dest. water - acetonitrile (95:5, v/v)
- Conditions
Eluent A: dest. water + 0,1 formic acid Eluent B: acetonitrile + 0,1 formic acid Gradient: 5 - 95 % B in 15 min, 95 % B for 5 min, 95 - 5 % B in 1 min, 5 % B for 9 min Flow rate: 0.30 mL/min Temperature: 40 °C Injection volume: 5 µL
- Detection
- LC-MS/MS AB Sciex API 5500 Ion source: Turbo Spray (ESI) Scan type: SRM Polarity: positive Curtain gas: 20 psig Ion spray voltage: 5500 V Temperature: 450 °C Gas 1 (nebulizer): 40 psig Gas 2 (turbo gas): 40 psig Collision gas: medium
- Note
- Author
- SPE department
- Source
- MACHEREY-NAGEL, Germany 2017
- Disclaimer
- Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products. MACHEREY-NAGEL does not warrant the correctness of the applications.
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