Photolytic transformation products and biological stability of the
hydrological tracer uranine
Photolytic transformation products and biological stability of the
hydrological tracer uranine
Photolytic transformation products and biological stability of the
hydrological tracer uranine
Application Number
127720
Method
HPLC
Results
Legend:
Chromatograms
A - total ion chromatogram of uranine after photo-treatment for 8.0 h
B-D - extracted ion chromatograms of Xe lamp generated transformation products
Peaks
UR - uranine
TP - transformation products
For photo-treatment of samples see the cited literature.
Conditions
Eluent A: 10 mmol/L ammonium acetate
Eluent B: acetonitrile
Gradient: 10 % B for 0.01 min, 10-30 % B in 4.99 min, 30-60 % B in 5 min, 60-10 % B in 3 min
Flow rate (LC-MS/MS): 0.7 mL/min
Flow rate (FLD): 1.0 mL/min
Temperature: 30 °C
Injection volume: 5 µL
Detection
LC-MS/MS
Flow rate (reduced with T cap): 0.35 mL/min
Mode: positive
Rt uranine: 6.3 min - see below chromatograms
FLD
476 nm / 515 nm
Rt uranine: 6.0 min - chromatogram was not published
Note
Author
Gutowski, L. et al.
Source
Science of the Total Environment 533 (2015) 446 - 453
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