Analysis of a PCB mixture

Analysis of a PCB mixture

Analysis of a PCB mixture

Application Number
215110
Method
GC
Results

Legend:
1 - 2,2',5-trichlorobiphenyl (PCB-18) 2 - 2,4',5-trichlorobiphenyl (PCB-28) 3 - 2,4,4'-trichlorobiphenyl (PCB-31) 4 - 2,2',5,5'-tetrachlorobiphenyl (PCB-52) 5 - 2,2',3,5-tetrachlorobiphenyl (PCB-43) 6 - 2,2',4,5,5'-pentachlorobiphenyl (PCB-101) 7 - 2,2',3,4',5',6-hexachlorobiphenyl (PCB-149) 8 - 2,3',4,4',5-pentachlorobiphenyl (PCB-123) 9 - 2,2',4,4',5,5'-hexachlorobiphenyl (PCB-153) 10 - 2,2',3,4,4',5'-hexachlorobiphenyl (PCB-138) 11 - 2,2',3,4,4',5,5'-heptachlorobiphenyl (PCB-180) 12 - 2,2',3,3',4,4',5,5'-octachlorobiphenyl (PCB-194)

Substances
2,2',5-trichlorobiphenyl (PCB-18); 2,4',5-trichlorobiphenyl (PCB-28); 2,4,4'-trichlorobiphenyl (PCB-31); 2,2',5,5'-tetrachlorobiphenyl (PCB-52); 2,2',3,5-tetrachlorobiphenyl (PCB-43); 2,2',4,5,5'-pentachlorobiphenyl (PCB-101); 2,2',3,4',5',6-hexachlorobiphenyl (PCB-149); 2,3',4,4',5-pentachlorobiphenyl (PCB-123); 2,2',4,4',5,5'-hexachlorobiphenyl (PCB-153); 2,2',3,4,4',5'-hexachlorobiphenyl (PCB-138); 2,2',3,4,4',5,5'-heptachlorobiphenyl (PCB-180); 2,2',3,3',4,4',5,5'-octachlorobiphenyl (PCB-194)
Product(s)
PhaseREFWebshop

OPTIMA 1701 MS

726630.30

Matrix
Sample(s)

100 ng/mL in hexane of each analyte

Conditions

Injection volume: 1.0 µL, splitless, after 1 min 1:50 Injection temperature: 250 °C Carrier gas: Helium, 42 cm/s Temperature: 100 °C --> [30 °C/min] --> 280 °C

Detection
MS Ionisation: EI Fullscan
Note
Author
GC department
Source
MACHEREY-NAGEL, Germany 2015
Disclaimer
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