Potential of HYDRODEX γ-TBDAc for enantiomer separation
Potential of HYDRODEX γ-TBDAc for enantiomer separation
Potential of HYDRODEX γ-TBDAc for enantiomer separation
- Application Number
- 214020
- Method
- GC
- Results
Legend:
points: The degree of separation obtained is evaluated using a points-based system (0 - 10 points), which considers the resolution and the level of difficulty. 0 points - no separation 1 - 5 points - partial separation 6 - 10 points - base line separation- Substances
- The following test substances were investigated for this study: 2-methylpentanol; 1-octen-3-ol; linalool; citronellol; 1-phenylethanol; indanol; menthol; methylbenzylamine (TFA); mandelic acid methyl ester; 1-phenylethanol (TFA); mecoprop methyl; 1-phenylpropanol (TFA); 2-phenylpropanol (TFA); mandelic acid methyl ester (TFA); rose oxide; linalool oxide; 2-phenylcyclohexanone; carvone; menthone; α-phenyl-γ-butyrolactone; α-ionone; citronellal; α-methyl-γ-butyrolactone; whiskey lactone; phenyloxirane; trans-stilbene oxide; α-pinene; limonene; theaspirane
- Product(s)
Phase REF Webshop HYDRODEX γ-TBDAc
723387.25
- Matrix
- Sample(s)
- Conditions
Carrier gas: hydrogen, 0.6 bar Split: 50 mL/min Temperature: 60 °C, 2 °C/min --> 200 °C
- Detection
- FID, 250 °C
- Note
- HYDRODEX γ-TBDAc shows good selectivities for esters, ketones, amides and derivatized alcohols (TFA esters) with a ring system close to the chiral C atom. For improved separations an optimization of the conditions is recommended. Please note: Successful separation of a test substance from a class of compounds will not guarantee a separation of a structurally similar compound. If you do not find an acceptable separation for the class of your compound please search for further applications or check the separation potential of HYDRODEX β-TBDAc in Appl. No. 214010 or LIPODEX E in Appl. No. 213960!
- Author
- GC department
- Source
- MACHEREY-NAGEL, Germany 2011
- Disclaimer
- Concerning questions to literature applications please contact the cited author/s. Chemicals mentioned in applications are not manufactured or sold by MACHEREY-NAGEL. Applications mentioned in MACHEREY-NAGEL literature or databases are provided for informational purposes only. MACHEREY-NAGEL does not warrant that all applications have been tested in MACHEREY-NAGEL laboratories using MACHEREY-NAGEL products. MACHEREY-NAGEL does not warrant the correctness of the applications.
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