Determination of Benzimidazole Anthelmintics in Meat Samples

Determination of Benzimidazole Anthelmintics in Meat Samples

Determination of Benzimidazole Anthelmintics in Meat Samples

Application Number
212040
Method
GC
Results
a)

Title: a)

Legend:
Chromatogram a) extract of kidney sample from a pig treated with fenbendazole, derivatized with pentafluorobenzyl bromide 1 + 2 - PFB derivatives of fenbendazole 3 + 4 - PFB derivatives of the metabolite fenbendazole sulphone Chromatogram b) extract of a blood sample from a pig treated with fenbendazole, derivatized with methyl iodide 1 + 2 - Me derivatives of fenbendazole 3 + 4 - Me derivatives of the metabolite fenbendazole sulphone 5 + 6 - Me derivatives of the metabolite oxfendazole


Substances
derivatives and metabolites of oxfendazole; fenbendazole and fenbendazole sulphone metabolites
Product(s)
PhaseREFWebshop

OPTIMA 1

726050.10

Matrix
meat
Sample(s)

Meat samples can be processed according to SPE Appl. No.: 304580.

Conditions

Injection: 1 µL, 270 °C Split: splitless Carrier gas: He, 1 mL/min Temperature: 60 °C (0.5 min) -> 150 °C, 30 °C/min -> 300 °C, 6°C/min

Detection
PND, 350 °C
Note
Author
Marti, A. M.; Mooser, A. E.; Koch, H.
Source
Journal of Chromatography, 498 (1990) 145-157
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